Ysi 9300 Photometer Manual do Utilizador

YSI 9300 and 9500 Photometers User Manual ®

7  Set the dilution factor to ‘On’ or ‘Off’. If the dilution factor option is set to ‘On’, the instrument will allow the entry of a numerical fact

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Oxygen is a major

Test Procedure 1 Filter sample if necessary to obtain a clear solution. 2 Fill the test tube with sample to the 10 ml mark. 3 Add one Sulfitest N

PHOTOMETER TEST INSTRUCTIONS ________________________________________________________________________________________ Zinc compounds are

SEPARATION OF RESIDUALS The photometer is programmed for both zinc and the copper correction procedure. Use program Phot 35 Zinc (+ Co

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ The Alkalinity of

Reagents and Equipment YSI Alkaphot M Tablets YSI Alkaphot P Tablets YSI 9300 or 9500 Photometer Round Test Tubes, 10 ml glass (PT 595) Test Proc

NOTE The expression of alkalinity results sometimes causes confusion. It is normal practice to express the result as mg/l CaCO3 (calcium c

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Iron occurs wide

Reagents and Equipment YSI Iron MR No 1 Tablets YSI Iron MR No 2 Tablets YSI Citrate IR Tablets YSI 9300 or 9500 Photometer Round Test Tubes, 10 ml

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Hydrazine is used a

8 Units The photometer offers the choice of result expressed in mg/l, ppm, mmol/l, µmol and g/l. Sample Number (9500 Only) A unique number may be

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Formulations c

Test Procedure 1 Filter sample if necessary to obtain a clear solution. 2 Fill test tube with sample to the 10 ml mark. 3 Add one Molybdate No 1

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Nitrites and nitrite

Test Procedure 1 Filter sample if necessary to obtain a clear solution. 2 Using the measuring syringe take 1 ml of the sample. Transfer to the tes

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ The use of organop

Reagents and Equipment YSI Oxidising OP Tablets YSI OP-A Tablets YSI OP-B Tablets YSI OP-AX Tablets YSI 9300 or 9500 Photometer YSI Test Tube, 20 ml

Test Procedure - Correction Factor If it is suspected that the sample contains orthophosphate, carry out the following correction procedu

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ The YSI Chloridol te

Reagents and Equipment YSI Acidifying CD Tablets YSI Chloridol Tablets YSI 9300 or 9500 Photometer Round Test Tubes,

5 Select the appropriate program number on the photometer for the test range required. 6 Take the photometer reading in usual manner (see photomet

9 Locking System Mode Settings (9500 Only) It is possible to 'lock’ the system settings so that these cannot be tampered with or altered a

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Pure water exhibits

Test Procedure 1 Filter sample through a GF/B filter paper. 2 Fill a test tube with filtered sample to the 10 ml mark. 3 Fill a test tube with de

PHOTOMETER TEST INSTRUCTIONS ________________________________________________________________________________________ Turbidity is an impo

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ The presence of d

Test Procedure Read the Oxygen test instructions leaflet contained in the CHEMetrics Vacu-Vials pack. Observe these various recommendations rega

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ DISSOLVED OXYGEN/

Test Procedure Read the Oxygen test instructions leaflet contained in the CHEMetrics Vacu-Vials pack. Observe these various recommendations rega

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ PHMB Polyhexamethylb

Test Procedure 1 Fill the test tube with sample to the 10 ml mark. 2 Add one PHMB-Phot tablet crush and mix to dissolve. 3 Select Phot 52 on phot

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Nickel does not occ

10 USB (9500 Only) The USB interface allows communication between the instrument and a PC. There is a choice of two operating modes – Hard Drive an

Test Procedure 1 Fill test tube with sample to the 10 ml mark. 2 Add one Nickeltest No 1 tablet, crush and mix to dissolve. Ensure tablet is compl

PHOTOMETER TEST INSTRUCTIONS ___________________________________________________________________________________________ Phenols and substi

Reagents and Equipment YSI Phenoltest No 1 Tablets YSI Phenoltest No 2 Tablets YSI Phenoltest PR Tablets YSI 9300 or 9500 Photometer Round Test

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Chromium may be pre

Reagents and Equipment For Hexavalent Chromium :- YSI Chromicol No 1 Tablets YSI Chromicol No 2 Tablets YSI 9300 or 9500 Photometer YSI Test Tube

Test Procedure - Total Chromium 1 Fill the pretreatment tube with sample to the 20 ml mark. 2 Add one level spoonful of Chromicol CR powder

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Silicon, in the

Test Procedure 1 Fill the test tube with sample to the 10 ml mark. 2 Add one Silica No 1 tablet, crush and mix to dissolve. 3 Add one Silica No 2

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Chlorine dioxide i

Important Note Chlorine dioxide is extremely volatile and can be lost from solution very easily. Extreme care must be taken when extracting and disp

11 4 INTERFACE CONNECTIONS AND DATA MEMORY (9500 ONLY) Stored data can be accessed by recall to the instrument display (see ‘View Log’). A

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Chlorine dioxide i

Important Note Chlorine dioxide is extremely volatile and can be lost from solution very easily. Extreme care must be taken when extracting and disp

Item # Y-PT 282 Rev A Drawing # Y-PT 282 © 2010 YSI IncorporatedV1-11/10

12 5 TAKING PHOTOMETER READINGS The photometer is very simple to use. Screen prompts guide the user towards the test result. The follo

13 The BLANK TUBE is a test tube filled only with the water being tested only. It is important to use the actual water to be tested to provide a tru

14 If the sample number option is pre-selected, then the following display will appear, for example (9500 only): Enter or confirm the sample num

15 3 The instrument will be set automatically. After a few seconds the following display will appear: Place SAMPLE TUBE in the test chamber

16 Continuation Tests (Certain Tests Only) 1 Select ‘Follow-On’ and press [OK] while the result is displayed of the currently running

YSI 9300 and 9500 Direct-Read Photometers User Manual YSI, Inc. 1725 Brannum Lane Yellow Springs, OH 45387 Tel: 800-897-4151 (+1 937-767-72

17 Reading in Transmittance and Absorbance When taking readings in Transmittance or Absorbance mode, use the  and  keys to step through the

18 To program user-defined calibrations: Turn the instrument ‘ON’, select ‘System’ menu and press [OK]. Scroll through the options to the USB entry

19 An example is shown below: USER CALIBRATION 900 Chlorine mmol/l 500nm Cl2 0,0 0.174,0.50 0.481,1.50 0.733,2.50 0.854,3.00 1.022,4.00 1.086,4.50 1

20 6 CARE AND MAINTENANCE The photometer is designed to give long and trouble-free operation. Care must be taken, however, to avoid

21 Photometer Up-Grade (9500 only) It is now possible to upgrade the photometer with new test calibrations using a computer. This will ensure that u

22 Limitation of Warranty This Warranty does not apply to any YSI product damage or failure caused by: 1 Failure to install, operate or use

Table of Contents Photometer Instructions PHOT.INST. TABLET REAGENT SYSTEM Alkalinity, Total (Alkaphot)

Direct-Reading Photometer Program Schedule TABLET REAGENT SYSTEM Instruction Sheet Number Reagent System Parameter Photometer Program Number - - Tr

Instruction Sheet Number Reagent System Parameter Photometer Program Number PHOT.23. Nitrate (Nitratest) Nitrate Nitrogen Phot 23 PHOT.24. Nitrite

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Natural and treat

INDEX 1 INTRODUCTION ... 1 Fe

Test Procedure 1 Fill test tube with sample to the 10 ml mark. 2 Add one Alkaphot tablet, crush and mix until all of the particles have dissolved.

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Aluminum sulphate is widel

Sample Collection Aluminum is readily absorbed on to the surfaces of sample containers, particularly glass containers. To avoid loss of aluminum, co

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Ammonia occurs as

Test Instructions 1 Fill test tube with sample to the 10 ml mark. 2 Add one Ammonia No 1 tablet and one Ammonia No 2 tablet, crush and mix to dis

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Bromine and brom

Reagents and Equipment YSI DPD No 1 Clear Tablets YSI DPD Nitrite Tablets YSI 9

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Chlorine and chlor

Reagents and Equipment YSI DPD No 1 Tablets YSI DPD No 2 Tablets YSI DPD No 3 Tablets YSI 9300 or 9500 Photometer Round Test Tu

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ CHLORINE DIOXIDE

1 1 INTRODUCTION The YSI 9300 and 9500 direct-read photometers are designed to give long and trouble-free operation. To ensure the best resul

Reagents and Equipment YSI DPD No 1 Tablets YSI DPD No 3 Tablets YSI DPD Glycine Tablets YSI DPD Acidifying Tablets YSI DPD Neutralising Tablets YSI

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Chlorine dioxide is

Reagents and Equipment YSI DPD No 1 Tablets YSI DPD No 3 Tablets YSI DPD Glycine Tablets YSI DPD Acidifying Tablets YSI DPD Neutralizing Tables YSI

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Chlorine and chlori

Reagents and Equipment YSI DPD No 1 Tablets YSI DPD Oxystop Tablets (Optional) YSI DPD No 3 Tablets YSI 9300 or 9500 Photometer Round Test Tubes,

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Chlorine and chlorine relea

Reagents and Equipment YSI DPD No 1 Tablets YSI DPD No 2 Tablets YSI DPD No 3 Tablets YSI 9300 or 9500 Photometer Round Test Tu

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ CHLORINE DIOXIDE

Reagents and Equipment YSI DPD No 1 Tablets YSI DPD No 3 Tablets YSI DPD Glycine Tablets YSI DPD Acidifying Tablets YSI DPD Neutralising Tablets YSI

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Chlorine dioxide i

2 Instrument Layout Test and Number Keys Multi-Size Cell Holder OK (Enter) Key Scroll and Selection Keys On/Off Key USB Interfac

Reagents and Equipment YSI DPD No 1 Tablets YSI DPD No 3 Tablets YSI DPD Glycine Tablets YSI DPD Acidifying Tablets YSI DPD Neutralizing Tables YSI

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Chlorine and chlorin

Reagents and Equipment YSI DPD No 1 Tablets YSI DPD Oxystop Tablets (Optional) YSI DPD No 3 Tablets YSI 9300 or 9500 Photometer Round Test Tubes,

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Chlorine and chlor

Test Instructions 1 Rinse test tube with sample leaving two or three drops of sample in the tube. 2 Add one DPD No 4 tablet, crush tablet and then

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Chlorine and chlo

Test Procedure 1 Fill test tube with sample to the 10 ml mark. 2 Add one Acidifying GP tablet and one Chlorine HR tablet. Crush tablets and mix to

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Copper occurs natu

Separation of Copper Residuals The direct-reading photometer is programmed for both free and total copper. Use program Phot 10 Free Copper, then

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Calcium hardness

3 Features and Technical Specification Application For application in general water testing using Palintest tablet reagent systems and Palin

Test Procedure 1 Filter sample if necessary to obtain a clear solution. 2 Fill the test tube with sample to the 10 ml mark. 3 Add one Calcicol No

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Cyanuric acid is

Test Procedure 1 Fill test tube with sample to the 10 ml mark. 2 Add one Cyanuric Acid tablet and allow to disintegrate for at least t

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Fluoride occurs n

TEST PROCEDURE 1 Fill test tube with sample to the 10 ml mark. 2 Add one Fluoride No 1 tablet, crush and mix to dissolve. 3 Add one Fluoride No 2

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Water hardness i

Test Procedure 1 Filter sample if necessary to obtain a clear solution. 2 Fill test tube with sample to the 10 ml mark. 3 Add one Hardicol No 1 t

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Hydrogen peroxide is

Test Procedure 1 Rinse test tube with sample leaving 2 to 3 drops of sample in the tube. 2 Add one Hydrogen Peroxide LR tablet, crush and then fi

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Hydrogen peroxide

4 2 OPERATING PRINCIPLE The YSI photometers are instruments that measure color intensity. Light is passed through a test tube containing

Test Procedure 1 Fill test tube with sample to the 10 ml mark. 2 Add one Acidifying PT tablet and one Hydrogen Peroxide HR tablet. Crush tablets

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Iron occurs widely

Reagents and Equipment YSI Iron LR Tablets YSI 9300 or 9500 Photometer Round Test Tubes 10 ml glass (PT 595) Test Procedure 1 Fill the test tube w

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Iron occurs widely i

Test Procedure 1 Fill test tube with sample to the 10 ml mark. 2 Add one Iron HR tablet, crush and mix to dissolve. 3 Stand for one minute to all

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Manganese-containi

Reagents and Equipment YSI Manganese No 1 Tablets YSI Manganese No 2 Tablets YSI 9300 or 9500 Photometer Round Test Tubes, 10 ml glass (PT 595)

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Magnesium is a

TEST PROCEDURE 1 Using the measuring syringe take a 1 ml sample of the water under test. Transfer to the round test tube and make up to t

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ MOLYBDATE HR Formu

5 Replacing the Batteries The battery compartment in the base of the instrument is secured by four screws. To replace the batteries, remove the cove

Reagents and Equipment YSI Molybdate No 1 HR Tablets YSI Molybdate No 2 HR Tablets YSI 9300 or 9500 Photometer Round Test Tubes, 10 ml glass (PT

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Nitrates are norm

Reagents and Equipment YSI Nitratest Powder (Spoon Pack) YSI Nitratest Tablets YSI Nitricol Tablets YSI Nitr

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Nitrites are foun

Test Procedure 1 Fill round test tube with sample to the 10 ml mark. 2 Add one Nitricol tablet, crush and mix to dissolve. 3 Stand for 10 minutes

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Ozone is used for

Reagents and Equipment YSI DPD No 4 Clear Tablets YSI DPD Glycine Tablets YSI 9300 or 9500 Photometer Round Test Tubes, 10 ml glass (PT 595) Se

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ pH measurement i

Notes 1 The color range of the phenol red test is yellow, through orange, to red. The formation of an intense purple coloration shows that the indi

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Phosphates are ex

6 3 GENERAL PHOTOMETER OPERATION The photometer is controlled by a simple intuitive menu system:  The highlight indicates the active line or se

Reagents and Equipment YSI Phosphate No 1 LR Tablets YSI Phosphate No 2 LR Tablets YSI 9300 or 9500 Photometer Round Test Tubes, 10 ml glass (PT

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Phosphates are ext

Test Procedure 1 Fill test tube with sample to the 10 ml mark. IN THE CASE OF SAMPLES CONTAINING SILICA (>20 mg/l SiO2) ONLY :- 2 Add one Phosp

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Potassium is an abu

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Silicon, in the

Test Instructions 1 Fill test tube with sample to the 10 ml mark 2 Add one Silica No 1 tablet, crush and mix to dissolve. Stand for five minutes t

PHOTOMETER TEST INSTRUCTIONS __________________________________________________________________________________________ Sulfates occur natu

Reagents and Equipment YSI Sulfate Turb Tablets YSI 9300 or 9500 Photometer Round Test Tubes, 10 ml glass (PT 595) Test Procedure 1 Fill test tube

PHOTOMETER TEST INSTRUCTIONS _________________________________________________________________________________________ Natural waters co

Sample Collection To prevent loss of sulphide collect the sample carefully with a minimum of agitation or aeration. Test the sample as s